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39
Subjective

Why is $\mathrm{NH}_2$ group of aniline acetylated before carrying out nitration?

Explanation

In order to check the activation of benzene ring by amino group, first it is acetylated with acetic anhydride or acetyl chloride in presence of pyridine to form acetanilide which can be further nitrated easily by nitrating mixture.

40
Subjective

What is the product when $\mathrm{C}_6 \mathrm{H}_5 \mathrm{CH}_2 \mathrm{NH}_2$ reacts with $\mathrm{HNO}_2$ ?

Explanation

$\mathrm{C}_6 \mathrm{H}_5 \mathrm{CH}_2 \mathrm{NH}_2$ on reaction with $\mathrm{HNO}_2$ produces $\mathrm{C}_6 \mathrm{H}_5 \mathrm{CH}_2 \mathrm{~N}_2^{+} \mathrm{Cl}^{-}$as follows

41
Subjective

What is the best reagent to convert nitrile to primary amine?

Explanation

Best reagent to convert nitrile to aniline is sodium/alcohol or $\mathrm{LiAlH}_4$.

42
Subjective

Give the structure 'A' in the following reaction.

Explanation

Complete conversion can be shown as

43
Subjective

What is Hinsberg reagent?

Explanation

Benzene sulphonyl chloride $\left(\mathrm{C}_6 \mathrm{H}_5 \mathrm{SO}_2 \mathrm{Cl}\right)$ is known as Hinsberg reagent. It is used to distinguish between primary, secondary and tertiary amine.